The Influence of Temperature on the Formation of Cubic Structured CdO Nanoparticles and Their Thin Films from Bis2-hydroxy-1-naphthaldehydatocadmiumII Complex via Thermal Decomposition TechniqueReportar como inadecuado




The Influence of Temperature on the Formation of Cubic Structured CdO Nanoparticles and Their Thin Films from Bis2-hydroxy-1-naphthaldehydatocadmiumII Complex via Thermal Decomposition Technique - Descarga este documento en PDF. Documentación en PDF para descargar gratis. Disponible también para leer online.

Journal of Nanotechnology - Volume 2017 2017, Article ID 8317109, 11 pages - https:-doi.org-10.1155-2017-8317109

Research Article

Department of Chemistry, Vaal University of Technology, P-Bag X021, Vanderbijlpark, South Africa

School of Materials, The University of Manchester, Oxford Rd, Manchester M139PL, UK

School of Chemistry, Wits University, Private Bag 3, Wits, Braamfontein 2025, South Africa

Correspondence should be addressed to Thokozani Xaba

Received 26 February 2017; Accepted 26 March 2017; Published 9 May 2017

Academic Editor: Andrey E. Miroshnichenko

Copyright © 2017 Thokozani Xaba et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

Recently, researchers have developed a great interest in the synthesis of metal oxide nanoparticles due to their potential applications in various fields of science and industry, especially in catalysis, due to their high activity. Bis2-hydroxy-1-naphthaldehydatocadmiumII complexes were prepared and used as precursors for the synthesis of cadmium oxide nanoparticles via thermal decomposition method using HDA as a stabilizing agent. The prepared complexes were also used as single source precursors to prepare CdO thin films onto the glass substrates by spin coating and were annealed at 250, 300, and 350°C, respectively. The precursors were characterized by Fourier transform infrared FTIR spectroscopy, elemental analysis, nuclear magnetic resonance NMR, and thermogravimetric analysis TGA. The synthesized CdO nanoparticles and CdO thin films were characterized by ultraviolet-visible UV-vis spectroscopy, photoluminescence PL, X-ray diffraction XRD, transmission electron microscopy TEM, scanning electron microscopy SEM, and atomic force microscopy AFM.





Autor: Thokozani Xaba, Makwena J. Moloto, Mohammad A. Malik, and Nosipho Moloto

Fuente: https://www.hindawi.com/



DESCARGAR PDF




Documentos relacionados