Z-N-3-2-Chloro-4-nitrophenyl-4-methylthiazol-23H-ylidene Pivalamide: Synthesis and Crystal StructureReportar como inadecuado




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Synthesis of the title compound was carried out by base-catalyzed cyclization of 1-pivaloyl-3-2-chloro-4-nitrophenyl thiourea with α-bromoacetone produced in situ. The structure was confirmed by the spectroscopic and elemental analysis and single crystal X-ray diffraction data. It crystallizes in the triclinic space group P-1 with unit cell dime sions a = 8.713710, b = 10.201014, c = 10.659313, α = 62.6719, β = 82.70110, γ = 79.76210, V = 827.218 ų, Z = 2.

KEYWORDS

Synthesis, 1-Pivaloyl-3-2-chloro-4-nitrophenyl Thiourea, Z-N-3-2-Chloro-4-nitrophenyl-4-methylthiazol-23H-ylidene Pivalamide, Crystal Structure

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A. Saeed and M. Bolte -Z-N-3-2-Chloro-4-nitrophenyl-4-methylthiazol-23H-ylidene Pivalamide: Synthesis and Crystal Structure,- Journal of Crystallization Process and Technology, Vol. 1 No. 3, 2011, pp. 41-48. doi: 10.4236-jcpt.2011.13007.





Autor: Aamer Saeed, Michael Bolte

Fuente: http://www.scirp.org/



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