Improvement of a Critical Intermediate Step in the Synthesis of a Nitroxide-Based Spin-Labeled Deoxythymidine AnalogReportar como inadecuado




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Department of Basic Pharmaceutical Sciences, West Virginia University School of Pharmacy, P. O. Box 9530, Morgantown, West Virginia, USA





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Abstract Methods to reduce the carboxylic acid moiety in 3-carboxy-2,2,5,5-tetramethylpyrrolin-1-oxyl to an alcohol as an intermediate toward the corresponding aldehyde have been explored and an improved method has been developed. View Full-Text

Keywords: Nitroxide; spin label; reduction; carboxylic acid; alcohol; anhydride Nitroxide; spin label; reduction; carboxylic acid; alcohol; anhydride





Autor: Jeannine H. Powell, Edward M. Johnson, II and Peter M. Gannett *

Fuente: http://mdpi.com/



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