10,10-Dimethoxy-9,9-biazuleno2,1-cphenanthreneReport as inadecuate


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Graduate School of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, Japan


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Abstract The title compound was prepared by the regioselective homocoupling of 10-methoxyazuleno2,1-cphenanthrene in the presence of ammonium persulfate. The structure of the synthesized compound was assigned on the basis of its 1H-NMR, FT-IR, and mass spectral data. Its crystal structure and electrochemical properties are also reported. View Full-Text

Keywords: azulene-fused helicene; homocoupling reaction; ammonium persulfate azulene-fused helicene; homocoupling reaction; ammonium persulfate

Author: Kosuke Yamamoto, Ryota Nakamae, Hiroshi Suemune * and Kazuteru Usui *

Source: http://mdpi.com/


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